Influence of the temperature and atmosphere in the sintering of hydroxyapatite

Authors

  • Juan Manuel Gonzalez Centre for Engineering and Industrial Development
  • Andrés Felipe Vásquez New Stetic S.A.
  • David González Federal University of São Carlos
  • Camilo Rivera University of Valle
  • Alexander Ruden Technological University of Pereira
  • Juan Pablo Trujillo Technological University of Pereira
  • Juan Manuel Alvarado Industrial Engineering and Development Center

DOI:

https://doi.org/10.17533/udea.rcm.n17a04

Keywords:

hidroxyapatite, granulometry, sintering

Abstract

In this work the effect of the temperature and sintering atmosphere of commercial Hydroxyapatite (HA) powder on its chemical composition, crystal structure, morphology and density is presented. Compacted HA samples of approximately 12 mm in diameter and ~0,3 g in weight were sintered at a temperature range between 900 and 1200 °C, with 100 °C increments, in atmospheres of air and argon. Regardless of the sintering atmosphere, the relative density increased with temperature, showing an increase in grain growth and reducing the open porosities. Additionally, an increase in mass loss was observed, with a higher effect for the argon atmosphere. As it is observed by infrared spectroscopy, the treatment in air allows the rehydration of the material in the cooling stage, while the analysis performed by X-ray diffraction demonstrated that the samples treated in argon showed a higher degree of dehydroxylation and decomposition to β-TCP from lower temperatures that for samples sintered in air
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Author Biographies

Juan Manuel Gonzalez, Centre for Engineering and Industrial Development

Ph.D. CONACYT-Center for Industrial Engineering and Development (CIDESI), Additive Manufacturing Consortium, (CONMAD), San Pablo Development, Querétaro, Mexico.

Andrés Felipe Vásquez, New Stetic S.A.

M.Sc. Research and Development at New Stetic S.A, Medellín, Colombia.

David González, Federal University of São Carlos

PhD Student in Materials Science and Engineering, Federal University of São Carlos (UFSCar), Brazil.

Camilo Rivera, University of Valle

Engineer, Hard Coatings and Industrial Applications Laboratory, University of Valle, Cali, Colombia.

Alexander Ruden, Technological University of Pereira

PhD Professor, Research Group: Biomedical Engineering and Forensic Sciences, Faculty of Basic Sciences, Technological University of Pereira, Risaralda, Colombia.

Juan Pablo Trujillo, Technological University of Pereira

M.Sc. Professor, Research Group: Biomedical Engineering and Forensic Sciences, Faculty of Basic Sciences, Technological University of Pereira, Risaralda, Colombia.

Juan Manuel Alvarado, Industrial Engineering and Development Center

PhD CONACYT-Center for Engineering and Industrial Development CIDESI, Additive Manufacturing Consortium, CONMAD, San Pablo Development, Querétaro, Mexico.

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Published

2021-09-15

How to Cite

Gonzalez, J. M., Vásquez, A. F., González, D., Rivera, C., Ruden, A., Trujillo, J. P., & Alvarado, J. M. (2021). Influence of the temperature and atmosphere in the sintering of hydroxyapatite. Revista Colombiana De Materiales, (17), 13. https://doi.org/10.17533/udea.rcm.n17a04

Issue

No. 17 (2021)

Section

Artículos

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Copyright (c) 2021 Revista Colombiana de Materiales

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