Optimization of a glass annealing process: a statistical and materials science approach to a glass containers manufacturing case application
DOI:
https://doi.org/10.17533/udea.rcm.336460Keywords:
lehr, annealing point, softening point, optical delay, birefringence and polarized lightAbstract
Annealing is one of the most important processes to manufacture glass since it provides relaxation to the SiO2 vitreous network and therefore it determines important mechanical properties required for doing this material useful. However, this process is also expensive due to there are involved high quantities of energy and time to carry it out, and for these reasons there is into the glass industry a paradigm regarding possible issues involved with the changing of variables to improve the process at the technical level without affecting the glass quality. In this order of ideas, progressive decreases of both, temperature and time were performed into an actual lehr, aiming to measure, to analyze and to compare the values of stress obtained from the actual and the proposed processes, all of this using the ASTM C336-71 and the ASTM C148-14 standards, as well as using statistical tools such as: Design of Experiments (DOE) and Analysis of Variance (ANOVA). As results were obtained non-significant statistical changes between the values of stress obtained for the majority of decreases performed, which allows to think about these decreases as an option for the high glass industry costs.
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J. Kim, J. Kong, K. Chung, “Analysis of annealing processes of glass sheets based on structural relaxation model”, International Journal of Mechanical Sciences, vol. 66, pp. 249 – 259, 2013.
J. M. Fernández, El Vidrio, Consejo Superior de Investigaciones Científicas de la Sociedad Española de Cerámica y Vidrio, Tercera Edición, Madrid, 2003.
Y. Ma, N. Wu, H. Zhang, S. Zhang, L. Zheng, “Thermal annealing system and process design to improve quality of large size glasses”, International Journal of Heat and Mass Transfer 72, pp. 411 – 422, 2014.
L. H. Adams, “The annealing of glass as a physical problem”, Geophysical Laboratory, Carnegie Institution of Washington, December, 1932.
J. T. Littleton, E. H. Roberts, “A method for determining the annealing temperature of glass”, Journal of the Optical Society of America, vol. 4, pp. 224 – 229, 1920.
H. R. Lillie, “Viscosity of glass between the strain point and melting temperature”, Journal of American Ceramic Society, pp. 502 – 514, 1931.
H. R. Lillie, “Re-Evaluation of glass viscosities at annealing and strain points”, Journal of American Ceramic Society, vol. 37, pp. 111 – 117, 1954.
D. A. McGraw, C. L. Babcock, “Effect of viscosity and stress level on rate of stress release in Soda-Lime, Potash-Barium and Borosilicate Glasses”, Journal of the American Ceramic Society, vol. 42, pp. 330 – 336, 1959.
ASTM C336 – 71, “Test method for annealing point and strain point of glass by fiber elongation”, 2015.
ASTM, C148 – 14, “Test methods for polariscopic examination of glass containers”, 2016.
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