The importance of RID and P Vs h curves on indentation studies of TiN films deposited onto M2 and 304L steels

Authors

  • J. M. Meza Universidad Pontificia Bolivariana
  • A. Devia Universidad Nacional de Colombia
  • J. M. Vélez Universidad Nacional de Colombia

DOI:

https://doi.org/10.17533/udea.redin.343444

Keywords:

mechanical properties, thin films, indentation, hardness, TiN, PAPVD

Abstract

A hardness study of TiN films onto M2 and 304L steels applied by PAPVD was conducted in this work. Instrumented indentation and hardness equipments allow to asses this property. Crack patterns produced during these tests were correlated with this information. In addition, from the P-h/t (Load-displacement/film’s thickness) plots, called Relative Indenter Displacement plots, and P-h plots important information was obtained about the capacity of these systems for supporting load. Both graphics showed to be of great importance for understanding the mechanical response of these systems to indentation.

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Author Biographies

J. M. Meza, Universidad Pontificia Bolivariana

Grupo de Nuevos Materiales. 

A. Devia, Universidad Nacional de Colombia

Laboratorio de Física del Plasma. 

J. M. Vélez, Universidad Nacional de Colombia

Grupo Ciencia y Tecnología de Materiales. 

References

C. Fisher, “Nanoindentation,” Springer, 2nd ed., 2004.

S. V. Hainsworth, M. R. McGurk, T. F. Page. “The effect of coating cracking on the indentation response of thin hard-coated systems”. Surf. Coat. Tech. Vol. 102. 1998. 97-107. DOI: https://doi.org/10.1016/S0257-8972(97)00683-X

A. M. Korsunsky, M. R. McGurk, S. J. Bull, T. F. Page. “On the hardness of coated systems”. Surf. Coat. Tech. Vol. 99. 1998. pp.171-183. DOI: https://doi.org/10.1016/S0257-8972(97)00522-7

M. R. McGurk, T. F. Page. “Using the P-δ2 analysis to deconvolute the nanoindentation response of hard-coated systems”. J. Mater. Res. Vol. 14. 1999. pp. 2283-2295. DOI: https://doi.org/10.1557/JMR.1999.0305

J. R. Tuck, A. M. Korsunsky, S. J. Bull, R. I. Davidson. “On the application of the work-of-indentation approach to depth-sensing indentation experiments in coated systems”. Surf. Coat. Tech. Vol. 137. 2001. pp. 217-224. DOI: https://doi.org/10.1016/S0257-8972(00)01063-X

J. R. Tuck, A. M. Korsunsky, D. G. Bhatc, S. J. Bull. “Indentation hardness evaluation of cathodic arc deposited thin hard coatings”. Surf. Coat. Tech. Vol. 139. 2001. pp 63-74. DOI: https://doi.org/10.1016/S0257-8972(00)01116-6

J. Loubet, J. Georges, G. Meille, In: Blau P. J:, Lawn B. R. (eds.). Microindentation Techniques in Materials science an Engineering ASTM STP 889. American Society for testing and Materials.Philadelphia. PA. 1986. pp. 72-89. DOI: https://doi.org/10.1520/STP32952S

A. Bolshakov, G. M. Pharr. “Influences of pile up on the measurement of mechanical properties by load and depth sensing indentation techniques”. J. Mater. Res. Vol. 13 1988. pp. 1049-1058. DOI: https://doi.org/10.1557/JMR.1998.0146

J. M. Meza, Jr. Franco., J. M. Vélez. “Calibration of nanoindentation equipment by means of Linear Method”. In preparation.

K. D. Bouzakis, N. Michaidilis, S. Hadjiyiannis, G. Erkens. “The effect of specimen roughness and indenter tip geometry on the determination accuracy of thin hard coatings stress-strain laws by nanoindentation”. Mater. Charact. Vol. 49. 2003. pp. 149-156. DOI: https://doi.org/10.1016/S1044-5803(02)00361-3

A. Leyland, A. Matthews, “On the significance of the H/E ratio in wear control: a nonocomposite coating approach to optimised tribological behaviour”. Wear Vol. 246. 2000. pp. 1-11. DOI: https://doi.org/10.1016/S0043-1648(00)00488-9

R. Yu Lo, D. Bogy. “Compensating for elastic deformation of the indenter in hardness test of very hard materials”. J. Mater. Res. Vol. 14. 1999. pp. 2276-2282. DOI: https://doi.org/10.1557/JMR.1999.0304

W. C. Oliver, G. M. Pharr. “An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments”. J. Mater. Res. Vol. 7. 1992. pp. 1564-83. DOI: https://doi.org/10.1557/JMR.1992.1564

X. Cay, H. Bangert. “Hardness measurements of thin films-determining the critical ratio of depth to thickness using FEM”. Thin Solid Films Vol. 264. 1995. pp. 59-71. DOI: https://doi.org/10.1016/0040-6090(95)06569-5

S. Bhowmick, A. Kale, V. Jayaram, S. K. Biswas. “Contact damage in TiN coating on steel”. Thin Solid Films. Vol. 436. 2003. pp. 250-258. DOI: https://doi.org/10.1016/S0040-6090(03)00598-4

J. M. Meza. “Applied indentation techniques to asses mechanical properties of TiN films”. MsC thesis. National University of Colombia. January. 2004.

A. G. Evans, E. Charles, “Fracture Toughness determination by indentation”. J. Amer Ceram. Soc. Vol. 59. 1976. pp. 371-372. DOI: https://doi.org/10.1111/j.1151-2916.1976.tb10991.x

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Published

2006-08-12

How to Cite

Meza, J. M., Devia, A., & Vélez, . J. M. (2006). The importance of RID and P Vs h curves on indentation studies of TiN films deposited onto M2 and 304L steels. Revista Facultad De Ingeniería Universidad De Antioquia, (37), 93–106. https://doi.org/10.17533/udea.redin.343444